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Chemical Structure| 756874-13-2 Chemical Structure| 756874-13-2

Structure of 756874-13-2

Chemical Structure| 756874-13-2

4-[(Methoxycarbonyl)(methyl)amino]butanoic acid

CAS No.: 756874-13-2

4.5 *For Research Use Only !

Cat. No.: A1122723 Purity: 95%

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Product Details of [ 756874-13-2 ]

CAS No. :756874-13-2
Formula : C7H13NO4
M.W : 175.18
SMILES Code : O=C(O)CCCN(C(OC)=O)C
MDL No. :MFCD11205651

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Application In Synthesis of [ 756874-13-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 756874-13-2 ]

[ 756874-13-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6976-17-6 ]
  • [ 79-22-1 ]
  • [ 756874-13-2 ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate; In 1,4-dioxane; water; at 20℃; for 16.0167h; 4- (Methylamino) butyric acid hydrochloride (5 g, 32.5 mmol), and potassium carbonate (18 g, 130 mmol) were suspended in water (50 ml) and dioxane (25 ml) then cooled to 0 oC. Methyl chloroformate (13 ml, 168 mmol) was added over 1 minute, then the mixture was stirred and allowed to warm slowly to room temperature for 16 hours. Conc. HC1 (20 ML) was added then the mixture was diluted with water and extracted with ethyl acetate. The organic layer was dried over magnesium sulfate, evaporated and dried in vacuo to give 4- [ (methoxycarbonyl) (methyl) amino] butyric acid as a thick clear oil (9.7 g).
 

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