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Chemical Structure| 75391-57-0 Chemical Structure| 75391-57-0

Structure of 75391-57-0

Chemical Structure| 75391-57-0

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Product Details of [ 75391-57-0 ]

CAS No. :75391-57-0
Formula : C10H11NO
M.W : 161.20
SMILES Code : N#CCC1=CC=C(OC)C(C)=C1
MDL No. :MFCD00040891

Safety of [ 75391-57-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H332-H335
Precautionary Statements:P261-P280-P305+P351+P338

Application In Synthesis of [ 75391-57-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 75391-57-0 ]

[ 75391-57-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 60736-71-2 ]
  • [ 143-33-9 ]
  • [ 75391-57-0 ]
  • 2
  • [ 773837-37-9 ]
  • [ 60736-71-2 ]
  • [ 75391-57-0 ]
YieldReaction ConditionsOperation in experiment
In dimethyl sulfoxide; N,N-dimethyl-formamide; at 20℃; for 16h; To a solution of <strong>[60736-71-2]4-(chloromethyl)-1-methoxy-2-methylbenzene</strong> (1.0 eq) in 1:1 DMSO/DMF (0.5M) was added NaCN (3.0 eq). The resulting mixture was stirred at r.t. for 16 h, then water was added and the mixture was extracted with EtOAc. The organic layer was washed with brine twice, dried over Na2SO4, concentrated under reduced pressure. The residue was purified by flash column chromatography (eluent: PE/EA=100:1 to 30:1) to give the title compound as a yellowish oil.
 

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