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Chemical Structure| 73537-92-5 Chemical Structure| 73537-92-5

Structure of 73537-92-5

Chemical Structure| 73537-92-5

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Product Details of [ 73537-92-5 ]

CAS No. :73537-92-5
Formula : C4H6N2O2
M.W : 114.10
SMILES Code : O=C([C@@H](N)C1)NC1=O
MDL No. :MFCD11894500

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Application In Synthesis of [ 73537-92-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 73537-92-5 ]

[ 73537-92-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 60846-91-5 ]
  • [ 73537-92-5 ]
YieldReaction ConditionsOperation in experiment
With hydrogen;5% palladium over charcoal; In methanol; under 1034.32 Torr; for 4h; Example -1; (3S)-3-(3-Cyclopentyloxy-4-methoxyphenylcarboxamido)-2,5-dioxoazolane. Step 1: (3S)-3-Aminoazolane-2,5-dione was prepared as follows: To a solution of (3S)-3-(N-Cbz-amino)azolane-2,5-dione ( 4.0 g, 16.12 mmol) in methanol (40 ml) was added 5 % palladium on carbon (50 mg) and was stirred under 20 psi 10 hydrogen pressure for 4 h. The mixture was filtered through a celite bed to remove the catalyst. The solvent was evaporated under reduced pressure to give 1.6 g of the product as pale yellow viscous liquid which was used as such for the next step.
 

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