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Chemical Structure| 7178-40-7 Chemical Structure| 7178-40-7

Structure of 7178-40-7

Chemical Structure| 7178-40-7

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Product Details of [ 7178-40-7 ]

CAS No. :7178-40-7
Formula : C11H15NO
M.W : 177.24
SMILES Code : CC1=CC=CC=C1N2CCOCC2
MDL No. :MFCD18251649

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Application In Synthesis of [ 7178-40-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7178-40-7 ]

[ 7178-40-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 110-91-8 ]
  • [ 615-37-2 ]
  • [ 7178-40-7 ]
YieldReaction ConditionsOperation in experiment
87% With sodium t-butanolate; In dimethyl sulfoxide; at 110℃; for 12h;Green chemistry; General procedure: Aryl halide (1.0 mmol), secondary amines (1mmol),2 mmol tBuONa and 0.2 mol% ofPd/Nf-G catalyst were addedin a 1 mL DMSO and the reaction was carried at 110C for 12h. The progress ofthe reaction was monitored by Gas Chromatography (GC). After completion ofreaction, the reaction mixture was cooled to room temperature and it was extracted with ethyl acetate. The catalyst was easily recovered by simple filtration followed by washing with ethanol and drying and preserved for nextruns. The pure products were obtained by column chromatography using hexane:ethyl acetate as the eluent. The preserved catalyst reused in a subsequent runfor recyclability study. The conversion of reactant was determined by Gaschromatography (GC).
 

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