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Chemical Structure| 71590-96-0 Chemical Structure| 71590-96-0

Structure of 71590-96-0

Chemical Structure| 71590-96-0

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Product Details of [ 71590-96-0 ]

CAS No. :71590-96-0
Formula : C8H7NO2
M.W : 149.15
SMILES Code : COC1=CC=CC(O)=C1C#N
MDL No. :MFCD16998786

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 71590-96-0 ]

[ 71590-96-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 16932-49-3 ]
  • [ 71590-96-0 ]
YieldReaction ConditionsOperation in experiment
In dimethyl sulfoxide; EXAMPLE 69: Preparation of N-[2-Hydroxy-3-(2-cyano-3-methoxyphenoxy)propyl]-1,1-dimethyl-2-(4-methoxyphenyl) ethylamine Hydrochloride, Compound 118 STR69 Powdered sodium cyanide (9.0 g, 184 mmol) and <strong>[16932-49-3]2,6-dimethoxybenzonitrile</strong> were added to 50 mL of dimethylsulfoxide and heated to 145 C. for 110 min under nitrogen. The reaction was cooled and poured into ether and dilute HCl. The ether layer was separated, washed twice with dilute acid, once with saturated brine, dried over anhydrous sodium sulfate, and concentrated. The yield of 2-cyano-3-methoxyphenol was 8.1 g.
 

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