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Chemical Structure| 68210-25-3 Chemical Structure| 68210-25-3

Structure of 68210-25-3

Chemical Structure| 68210-25-3

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Product Details of [ 68210-25-3 ]

CAS No. :68210-25-3
Formula : C7H10N2O
M.W : 138.17
SMILES Code : OC1=NC(C(C)C)=NC=C1
MDL No. :MFCD03453289

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Application In Synthesis of [ 68210-25-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 68210-25-3 ]

[ 68210-25-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 34846-90-7 ]
  • [ 22007-68-7 ]
  • [ 68210-25-3 ]
YieldReaction ConditionsOperation in experiment
84% With potassium carbonate; In ethanol; at 85℃; for 10h; The mixture of methyl 3-methoxyacrylate (4.0g, 34.4mmol), isobutyrimidamide hydrochloride (12.64g, 103.2 mmol) and potassium carbonate (15.2g, 110.1 mmol) in ethanol (50 mL) was stined at 85 °C for 10h. The reaction mixture was filtered through a pad of celite. The filtrate was evaporated under reduced pressure to get 2-isopropylpyrimidin-4(3H)-one (4.0g,84percent). ?H NMR (400 MHz, DMSO-d6): oe 12.37 (br s, 1H), 7.84 (d, J= 6.6 Hz, 1H), 6.14 (d, J=6.6 Hz, 1H), 2.71 ? 2.83 (m, 1H), 0.97 (d, J= 6.9 Hz, 6H)); LC-MS: 138.9 [M+H].
 

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