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CAS No. : | 66949-81-3 | MDL No. : | MFCD11849273 |
Formula : | C13H11ClFN | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | RPANWYSQFQHEEP-UHFFFAOYSA-N |
M.W : | 235.68 | Pubchem ID : | 61382680 |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P280-P301+P312-P302+P352-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With phenol at 125 - 130℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
/BRN= 457539/ (I-2), PCl5/POCl3; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In pentan-1-ol at 137℃; for 24h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: sodium hydroxide / water / 20 °C 2: trichlorophosphate / neat (no solvent) / 115 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With trichlorophosphate In neat (no solvent) at 115℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: sodium iodide / pentan-1-ol / 137 °C 2: potassium carbonate / tetrahydrofuran / 66 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: sodium iodide / pentan-1-ol / 137 °C 2: potassium carbonate / tetrahydrofuran / 66 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: sodium iodide / pentan-1-ol / 137 °C 2: potassium carbonate / tetrahydrofuran / 66 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: sodium iodide / pentan-1-ol / 137 °C 2: potassium carbonate / tetrahydrofuran / 66 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1.1: pentan-1-ol / 24 h / 137 °C 2.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C 2.2: 1 h / 20 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: sodium iodide / pentan-1-ol / 137 °C 2: potassium carbonate / tetrahydrofuran / 66 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sodium iodide In pentan-1-ol at 137℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sodium iodide In pentan-1-ol at 137℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sodium iodide In pentan-1-ol at 137℃; |