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Chemical Structure| 6279-88-5 Chemical Structure| 6279-88-5

Structure of 6279-88-5

Chemical Structure| 6279-88-5

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Product Details of [ 6279-88-5 ]

CAS No. :6279-88-5
Formula : C12H12O2
M.W : 188.22
SMILES Code : O=C(C1=C(C)C2=C(C=CC=C2)CC1)O
MDL No. :MFCD20638405

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Application In Synthesis of [ 6279-88-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6279-88-5 ]

[ 6279-88-5 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 5337-63-3 ]
  • [ 6279-88-5 ]
YieldReaction ConditionsOperation in experiment
81% Aceto-alpha-phenyl-gamma-butyric acid ethyl ester (5 g, 27 mmol) was added dropwise to H2SO4 (30 mL) at -20C. The mixture is stirred at this temperature for 4 h and was then cautiously hydrolyzed in of a cold water (300 mL). The white precipitate was filtered of and dried overnight. The crude acid was recrystallized with a benzene-hexane mixture to yield white crystals (81%. mp. 127C). 1H NMR (200 MHz, CDCl3): delta 2.57 (s, 3 H), 2.63-2.68 (m, 2 H), 2.77-2.81 (m, 2 H), 7.17-7.53 (m, 4 H).
  • 2
  • [ 7664-93-9 ]
  • [ 5337-63-3 ]
  • [ 6279-88-5 ]
  • 3
  • [ 7664-93-9 ]
  • [ 5337-63-3 ]
  • [ 6279-88-5 ]
  • [ 4488-44-2 ]
 

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