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Chemical Structure| 62265-67-2 Chemical Structure| 62265-67-2

Structure of 62265-67-2

Chemical Structure| 62265-67-2

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Product Details of [ 62265-67-2 ]

CAS No. :62265-67-2
Formula : C11H11Cl2NO2
M.W : 260.12
SMILES Code : OC1=CC2=C(N(C(C(Cl)Cl)=O)CCC2)C=C1

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Application In Synthesis of [ 62265-67-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 62265-67-2 ]

[ 62265-67-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 79-36-7 ]
  • [ 3373-00-0 ]
  • [ 107-06-2 ]
  • [ 62265-67-2 ]
YieldReaction ConditionsOperation in experiment
In hexane; chloroform; A-1. 1-(Dichloroacetyl)-<strong>[3373-00-0]1,2,3,4-tetrahydro-6-quinolinol</strong> -- To a stirred mixture containing 14.9 g. of <strong>[3373-00-0]1,2,3,4-tetrahydro-6-quinolinol</strong> and 250 ml. of dry ethylene dichloride was added dropwise 16.2 g. of dichloroacetyl chloride and the resulting reaction mixture was stirred on a steam bath for fourteen hours. The reaction mixture was heated in vacuo to remove the ethylene dichloride. The remaining material was taken up in chloroform and the chloroform removed in vacuo to yield 28 g. of powder. The powder was slurried at room temperature with 100 ml. of n-hexane containing 10 ml. of isopropyl alcohol and the remaining solid, 24.5 g., was recrystallized twice from chloroform-n-hexane and dried at 60 C. and 0.1 mm. for seven hours to yield 10.5 g. of 1-(dichloroacetyl)-<strong>[3373-00-0]1,2,3,4-tetrahydro-6-quinolinol</strong>, m.p. 136-136.5 C.
 

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