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Chemical Structure| 6214-47-7 Chemical Structure| 6214-47-7

Structure of 6214-47-7

Chemical Structure| 6214-47-7

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Product Details of [ 6214-47-7 ]

CAS No. :6214-47-7
Formula : C8H9ClN2O2
M.W : 200.62
SMILES Code : O=C(OCC)CC1=CN=CN=C1Cl
MDL No. :MFCD13194669
InChI Key :HEDARYMFTQTCTI-UHFFFAOYSA-N
Pubchem ID :46856293

Safety of [ 6214-47-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H332-H335
Precautionary Statements:P261-P280-P305+P351+P338

Application In Synthesis of [ 6214-47-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6214-47-7 ]

[ 6214-47-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6214-46-6 ]
  • [ 6214-47-7 ]
YieldReaction ConditionsOperation in experiment
79% With trichlorophosphate; for 2h;Reflux; General procedure: A mixture of compound 1 (X = H, Me, Ph, SMe; Y = H,R1 = Et) and phosphoryl chloride was refluxed for 2 h.Phosphoryl chloride was then evaporated. Dichloromethane(DCM) and water was added to the dark oilyresidue. It was cooled to 5-10 C and ammonium hydroxidesolution was added until pH 9-10. The layers wereseparated and the aqueous layer was extracted with DCM.The combined organic layer was washed with aqueousNaHCO3 solution (10 %) and brine. It was dried andevaporated to give compounds 7
 

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