Home Cart Sign in  
Chemical Structure| 60070-05-5 Chemical Structure| 60070-05-5

Structure of 60070-05-5

Chemical Structure| 60070-05-5

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 60070-05-5 ]

CAS No. :60070-05-5
Formula : C10H14O2
M.W : 166.22
SMILES Code : OCC1=CC(C)=C(C)C=C1CO
MDL No. :MFCD00597998
InChI Key :VSODREOTHFONSP-UHFFFAOYSA-N
Pubchem ID :7020684

Safety of [ 60070-05-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H332-H302
Precautionary Statements:P261-P264-P270-P271-P301+P312+P330-P304+P340+P312-P501

Application In Synthesis of [ 60070-05-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 60070-05-5 ]

[ 60070-05-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 17649-59-1 ]
  • [ 60070-05-5 ]
YieldReaction ConditionsOperation in experiment
100% Preparation of 1,2-bis(bromomethyl)-4,5-dimethylbenzene Dried tetrahydrofurane (20 mL) was put into LAH (0.54 g, 14.29 mmol) at -78 C. Dimethyl 4,5-dimethylbenzene-1,2-dicarboxylate (1.27 g, 5.71 mmol) was dissolved in dried tetrahydrofurane (10 mL), and then the resultant mixture was slowly added into the above reaction solution. Then the reaction temperature was slowly raised to room temperature, and then stirring under reflux was performed for 24 hours. After the reaction, the resultant reaction material was cooled by a sodium hydroxide solution, and then concentrated under reduced pressure, followed by washing with ethyl acetate twice and again washing with distilled water once. The organic layer was separated, and dried over sodium sulfate, and then the solvent was concentrated under reduced pressure, thereby obtaining white solids, (4,5-dimethyl-1,2-phenylene)dimethanol (0.95 g, quantitative). This is subjected to a bromination reaction using tribromophosphine, thereby obtaining 1,2-bis(bromomethyl)-4,5-dimethyl benzene at a yield of 56%. 1H-NMR 300 MHz (CDCl3) δ 7.13 (s, 2H), 4.27 (s, 4H), 2.23 (s, 6H).
 

Historical Records

Technical Information

Categories

Related Functional Groups of
[ 60070-05-5 ]

Aryls

Chemical Structure| 16308-92-2

A165671 [16308-92-2]

(2,4-Dimethylphenyl)methanol

Similarity: 1.00

Chemical Structure| 13651-14-4

A234784 [13651-14-4]

(2,3-Dimethylphenyl)methanol

Similarity: 1.00

Chemical Structure| 4170-90-5

A282259 [4170-90-5]

Mesitylmethanol

Similarity: 1.00

Chemical Structure| 62285-58-9

A344600 [62285-58-9]

(2,6-Dimethylphenyl)methanol

Similarity: 1.00

Chemical Structure| 484-66-2

A708770 [484-66-2]

(2,3,4,5,6-Pentamethylphenyl)methanol

Similarity: 1.00

Alcohols

Chemical Structure| 16308-92-2

A165671 [16308-92-2]

(2,4-Dimethylphenyl)methanol

Similarity: 1.00

Chemical Structure| 13651-14-4

A234784 [13651-14-4]

(2,3-Dimethylphenyl)methanol

Similarity: 1.00

Chemical Structure| 4170-90-5

A282259 [4170-90-5]

Mesitylmethanol

Similarity: 1.00

Chemical Structure| 62285-58-9

A344600 [62285-58-9]

(2,6-Dimethylphenyl)methanol

Similarity: 1.00

Chemical Structure| 484-66-2

A708770 [484-66-2]

(2,3,4,5,6-Pentamethylphenyl)methanol

Similarity: 1.00