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Chemical Structure| 5837-73-0 Chemical Structure| 5837-73-0
Chemical Structure| 5837-73-0

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Methyl 2-hydroxybut-3-enoate

CAS No.: 5837-73-0

4.5 *For Research Use Only !

Cat. No.: A772660 Purity: 95%

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Product Details of [ 5837-73-0 ]

CAS No. :5837-73-0
Formula : C5H8O3
M.W : 116.12
SMILES Code : C=CC(O)C(OC)=O
MDL No. :MFCD00144164

Safety of [ 5837-73-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis [ 5837-73-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5837-73-0 ]

[ 5837-73-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 67-56-1 ]
  • sucrose [ No CAS ]
  • [ 530-26-7 ]
  • [ 27871-49-4 ]
  • [ 1663-35-0 ]
  • [ 5837-73-0 ]
  • [ 1186-47-6 ]
  • [ 56-82-6 ]
  • [ 621-63-6 ]
YieldReaction ConditionsOperation in experiment
72% With potassium carbonate; at 160℃; for 16h;Flow reactor; The stainless steel pressure vessel (40 cc, Swagelok) is filled in with the methanol (15.0 g: Sigma-Aldrich, 003e99.8percent) solution of the metal salt (metal ion supply source), and sucroses (0.450 g: Fluka, 003e99.0percent) and catalyst (0.150 g). The reactor is closed and it heats up under the mixing (700 rpm) with 160. In 160 reaction, it makes maintained for 16 hours and the container reaction rapidly is cooled in the cold water after this period as the dipping. Sample from the reaction container was filtered and it analyzed with the HPLC (the Agilent 1200, the Biorad Aminex HPX-87H column, 65, 0.05 M H2SO4, 0.6 ml min-1) and it was the art exhibition ring hexose and dihydroxy acetone (DHA), the methyllactate (ML) using the fixed quantity: and GC (the Agilent 7890 in which the Phenomenex Solgelwax column is comprehended) the glyceraldehyde (GLA), and methyl vinyl glycol rate (MVG, and the methyl 2- hydroxy -3- butenoate) and glycol aldehyde dimethylacetal (GADMA) the fixed quantity.
 

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