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Chemical Structure| 5806-58-6 Chemical Structure| 5806-58-6

Structure of 5806-58-6

Chemical Structure| 5806-58-6

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Product Details of [ 5806-58-6 ]

CAS No. :5806-58-6
Formula : C20H22
M.W : 262.39
SMILES Code : CC1=CC(C)=CC(C)=C1C#CC2=C(C)C=C(C)C=C2C

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Application In Synthesis of [ 5806-58-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5806-58-6 ]

[ 5806-58-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 4028-63-1 ]
  • [ 1066-54-2 ]
  • [ 769-26-6 ]
  • [ 5806-58-6 ]
YieldReaction ConditionsOperation in experiment
11%; 74% General procedure: 4-Iodoanisole (1mmol), TMSA (1.1mmol) and K2CO3 (2mmol) were added to a freshly prepared solution of PdNPs (5mL) in a 25mL round bottomed flask fitted with stopper. Then, the reaction mixture was stirred at 40C. The reaction progress was monitored by TLC, until complete consumption of aryl iodide. To the reaction mixture containing in situ formed 4-ethynylanisole the next batch of aryliodide (1mmol) was added and the reaction mixture was further allowed to stir until complete consumption of the arylacetylene. In this manner the targeted unsymmetrical diarylacetylene was formed. The detailed procedure is provided in the Supp. Info. Detailed procedure for synthesis of symmetrical diarylacetylenes is also mentioned in SI.
 

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