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Chemical Structure| 570390-94-2 Chemical Structure| 570390-94-2

Structure of 570390-94-2

Chemical Structure| 570390-94-2

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Product Details of [ 570390-94-2 ]

CAS No. :570390-94-2
Formula : C8H16ClNO3
M.W : 209.67
SMILES Code : O=C(OC(C)(C)C)NCC(O)CCl
MDL No. :MFCD18974014

Safety of [ 570390-94-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 570390-94-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 570390-94-2 ]

[ 570390-94-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 34619-03-9 ]
  • [ 62037-46-1 ]
  • [ 570390-94-2 ]
  • 2
  • [ 24424-99-5 ]
  • [ 62037-46-1 ]
  • [ 570390-94-2 ]
YieldReaction ConditionsOperation in experiment
96.71% With sodium hydrogencarbonate; In methanol; water; at 20℃; for 3h; The reaction flask was charged with 116.8 g of compound II (0.80 mol)191.8 g of Boc2O (0.88 mol) and 1500 ml of methanol, stirred,And 1200 ml of an aqueous solution containing 80.6 g of sodium hydrogencarbonate (0.96 mol)And then reacted at room temperature for 3 hours. After the reaction was complete, the methanol was removed by concentration,The residue was extracted with 2000 ml of methylene chloride and the dichloromethane layer was washed with water,And finally dried over anhydrous sodium sulfate; filtered, the filtrate was concentrated to dryness,174.3 g of an oil was obtained, and 1200 ml of petroleum ether was added to the oil to freeze the crystals,The filter cake was washed with petroleum ether to give 161.7 g of the white solid, compound III; mp 48-51 C, molar yield: 96.71% (calculated as compound II).
 

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