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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 55745-68-1 Chemical Structure| 55745-68-1

Structure of 55745-68-1

Chemical Structure| 55745-68-1

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Product Details of [ 55745-68-1 ]

CAS No. :55745-68-1
Formula : C9H9ClO
M.W : 168.62
SMILES Code : ClCC1=CC=C(OCC2)C2=C1
MDL No. :MFCD09261153

Safety of [ 55745-68-1 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314-H290
Precautionary Statements:P501-P260-P234-P264-P280-P390-P303+P361+P353-P301+P330+P331-P363-P304+P340+P310-P305+P351+P338+P310-P406-P405
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 55745-68-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 55745-68-1 ]

[ 55745-68-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 103262-35-7 ]
  • [ 55745-68-1 ]
  • 2
  • [ 103262-35-7 ]
  • [ 124-63-0 ]
  • [ 55745-68-1 ]
YieldReaction ConditionsOperation in experiment
100% With triethylamine; In dichloromethane; ethyl acetate; Reference Example 14-1 (2,3-dihydrobenzo[b]furan-5-yl)methyl chloride To a solution of <strong>[103262-35-7](2,3-dihydrobenzo[b]furan-5-yl)methanol</strong> (1.5 g, 10 mmol) in dichloromethane (10 mL) were added under ice-cooling triethylamine (1.67 mL, 12 mmol) and methanesulfonyl chloride (0.85 mL, 10 mmol) and the mixture was stirred at room temperature for 1 h. The solvent was evaporated under reduced pressure and the obtained residue was dissolved in ethyl acetate. The organic layer was washed with saturated brine and dried over anhydrous sodium sulfate. The solvent was evaporated under reduced pressure to give an almost pure title compound (1.6 g, 100%).
 

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