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[ CAS No. 55618-86-5 ] {[proInfo.proName]}

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Chemical Structure| 55618-86-5
Chemical Structure| 55618-86-5
Structure of 55618-86-5 * Storage: {[proInfo.prStorage]}
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Product Details of [ 55618-86-5 ]

CAS No. :55618-86-5 MDL No. :MFCD00435229
Formula : C15H15NO2 Boiling Point : -
Linear Structure Formula :- InChI Key :UIINMWIYQHIFQH-UHFFFAOYSA-N
M.W : 241.29 Pubchem ID :4178998
Synonyms :

Safety of [ 55618-86-5 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 55618-86-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 55618-86-5 ]

[ 55618-86-5 ] Synthesis Path-Downstream   1~10

YieldReaction ConditionsOperation in experiment
entspr. Saeure, CH2N2;
1,2,3,4-Tetrahydro-acridin-9-carbonsaeure, DMS, NaOMe/Me., Δ;
  • 2
  • [ 74-88-4 ]
  • [ 55618-86-5 ]
YieldReaction ConditionsOperation in experiment
With methanol
  • 5
  • [ 55618-86-5 ]
  • 8-(1,2,3,4-tetrahydro-9-acridine-9-yl)oct-7-enenitrile [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: 64 percent / DIBAL-H / toluene / 2 h / -78 °C 2.1: t-BuOK / tetrahydrofuran / 0.5 h / -78 °C 2.2: 73 percent / tetrahydrofuran / -78 - 20 °C
  • 6
  • [ 55618-86-5 ]
  • 8-(1,2,3,4-tetrahydro-9-acridine-9-yl)-7-octenyl-1-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1.1: 64 percent / DIBAL-H / toluene / 2 h / -78 °C 2.1: t-BuOK / tetrahydrofuran / 0.5 h / -78 °C 2.2: 73 percent / tetrahydrofuran / -78 - 20 °C 3.1: 86 percent / LiAlH4 / diethyl ether / 2 h / 20 °C
  • 7
  • [ 55618-86-5 ]
  • N-(1,2,3,4-tetrahydro-9-acridine-9-yl)-N-[8-(1,2,3,4-tetrahydroacridin-9-yl)oct-7-en-1-yl]amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1.1: 64 percent / DIBAL-H / toluene / 2 h / -78 °C 2.1: t-BuOK / tetrahydrofuran / 0.5 h / -78 °C 2.2: 73 percent / tetrahydrofuran / -78 - 20 °C 3.1: 86 percent / LiAlH4 / diethyl ether / 2 h / 20 °C 4.1: 35 percent / pentan-1-ol / 12 h / 160 °C
  • 8
  • [ 55618-86-5 ]
  • (1,2,3,4-tetrahydro-acridin-9-yl)-[8-(1,2,3,4-tetrahydro-acridin-9-yl)-octyl]-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 5 steps 1.1: 64 percent / DIBAL-H / toluene / 2 h / -78 °C 2.1: t-BuOK / tetrahydrofuran / 0.5 h / -78 °C 2.2: 73 percent / tetrahydrofuran / -78 - 20 °C 3.1: 86 percent / LiAlH4 / diethyl ether / 2 h / 20 °C 4.1: 35 percent / pentan-1-ol / 12 h / 160 °C 5.1: 92 percent / H2 / Pd/C / methanol / 4 h / 20 °C / 2068.59 Torr
  • 9
  • [ 38186-54-8 ]
  • [ 74-88-4 ]
  • [ 55618-86-5 ]
YieldReaction ConditionsOperation in experiment
72% With potassium carbonate In acetone for 5h; Reflux; 5.1.2.2. Methyl 6-chloro-2-(4-methoxyphenyl) quinoline-4-carboxylate (3a) General procedure: 6-Chloro-2-(4-methoxyphenyl) quinoline-4-carboxylic acid (2a) (0.98 g, 3 mmol) and potassium carbonate (2.07 g, 15 mmol) were weighed into a round-bottom flask. Methyl iodide (0.95 mL, 15 mmol) and acetone (4 mL) were added. The reaction mixture was refluxed with magnetic stirring. The progress of the reaction was monitored by TLC. The reaction was completed after 5 h. The solvent was evaporated in vacuo and water was added to the remaining mixture. The product was collected by suction filtration and air-dried. The crude product was separated on a silica gel column to obtain pure 3a at 90% yield.
  • 10
  • [ 91-56-5 ]
  • [ 108-94-1 ]
  • [ 55618-86-5 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: potassium hydroxide / 0.5 h / Reflux 1.2: 20 h / Reflux 2.1: potassium carbonate / acetone / 5 h / Reflux
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