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Chemical Structure| 54323-50-1 Chemical Structure| 54323-50-1

Structure of 54323-50-1

Chemical Structure| 54323-50-1

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Product Details of [ 54323-50-1 ]

CAS No. :54323-50-1
Formula : C6H9NO3S
M.W : 175.21
SMILES Code : O=C([C@H]1N(C(C)=O)CSC1)O
MDL No. :MFCD00038440
InChI Key :WXTBYSIPOKXCPM-YFKPBYRVSA-N
Pubchem ID :197107

Safety of [ 54323-50-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 54323-50-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 54323-50-1 ]

[ 54323-50-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 50-00-0 ]
  • [ 108-24-7 ]
  • [ 207121-46-8 ]
  • [ 54323-50-1 ]
YieldReaction ConditionsOperation in experiment
96% With sodium carbonate; In water; at 20 - 50℃; for 1h;pH 7 - 10;Large scale; 250 kg of tap water, 60 kg of 37% formaldehyde solution and 100 kg of <strong>[207121-46-8]L-cysteine hydrochloride monohydrate</strong> were added to a 500 liter reactor, and the mixture was clarified by stirring at room temperature.The saturated sodium carbonate solution is added dropwise to maintain the pH of the reaction system in the range of 7-10.After detecting the raw material reaction, the plate is heated to 50 C, and acetic anhydride and saturated sodium carbonate solution are added dropwise.The pH of the reaction system was maintained in the range of 7 to 10. After the completion of the dropwise addition, the reaction was continued for 1 hour.After the plate material is detected to be completely reacted, concentrated hydrochloric acid is added dropwise to adjust the pH of the system to 5-6, and add activated carbon 20 kg.Decolorization by heating, back-filtering of the plate frame,The filtrate was diluted with hydrochloric acid to adjust the pH to 1-2, and the mixture was slowly stirred and crystallized.Centrifuge the precipitated solid, dry, package,96 kg of bright white granular acetylthioproline solid was obtained in a yield of 96%.
 

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