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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 54127-64-9 Chemical Structure| 54127-64-9

Structure of 54127-64-9

Chemical Structure| 54127-64-9

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Product Details of [ 54127-64-9 ]

CAS No. :54127-64-9
Formula : C7H9ClN2
M.W : 156.61
SMILES Code : ClC1=CC=C(CCN)C=N1
MDL No. :MFCD08449285
InChI Key :DSJPCYWXUGROQW-UHFFFAOYSA-N
Pubchem ID :20483490

Safety of [ 54127-64-9 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H335-H314
Precautionary Statements:P260-P264-P270-P271-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P363-P403+P233-P405-P501
Class:8
UN#:2735
Packing Group:

Application In Synthesis of [ 54127-64-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 54127-64-9 ]

[ 54127-64-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 433336-90-4 ]
  • [ 54127-64-9 ]
YieldReaction ConditionsOperation in experiment
Intermediate 33; 2-(6-Chloropyridin-3-yl)-ethanamine; To 2.00 g (11.7 mmol) <strong>[433336-90-4]2-(6-chloropyridin-3-yl)-acetamide</strong> in 50 mL THF at 0 C. are added 12.9 ml LAH (c=1 mol/l in THF) by a dropping funnel. Cooling is removed and the reaction mixture is stirred for 1 h at r.t., then 8 ml LAH (c=1 mol/l in THF) are added and the reaction mixture is stirred at r.t. over night. The reaction is carefully quenched by the addition of 2 ml of an aq. NaHCO3 solution (10%). The mixture is filtrated and the solvent is removed under reduced pressure. The crude product is used without further purification.C7H9ClN2 (M=156.6 g/mol)ESI-MS: 157 [M+H]+ Rt (HPLC): 1.12 min (method AB)
 

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