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Chemical Structure| 5333-61-9 Chemical Structure| 5333-61-9

Structure of 5333-61-9

Chemical Structure| 5333-61-9

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Product Details of [ 5333-61-9 ]

CAS No. :5333-61-9
Formula : C13H18O
M.W : 190.28
SMILES Code : OC1C(CC2=CC=CC=C2)CCCC1

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Application In Synthesis of [ 5333-61-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5333-61-9 ]

[ 5333-61-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 120-32-1 ]
  • [ 28994-41-4 ]
  • [ 5333-61-9 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; In water; at 20℃; General procedure: Experiments were carried out in 250-cm3 round flasks on amagnetic stirrer equipped with StarFish attachment (RadleysDiscovery Technologies, UK) which enables to performfive different experiments at the same time and at thesame ambient conditions. All experiments were carried out in air at ambient temperature (20-25 C). All used solutionswere prepared in distilled water. Stock solutions of 1or 2 were prepared in concentrations of 10 mmol dm-3 inaqueous solution of appropriate base (salt, respectively).To the 10 mmol dm-3 solution of studied 1 or 2 dissolvedin 100 mmol dm-3 of base, the appropriate amount oftested alloy (Al-Ni, Devarda?s, Arnd?s) was added. Theflask with the reaction mixture was closed with glass tubefilled with granulated charcoal and the reaction mixtureswere stirred at 350 rpm at ambient temperature (20-25 C)for approximately 21 h and filtered subsequently. Obtainedfiltrate was acidified using 18% H2SO4 to pH around 3,then transferred into the separation funnel and extractedwith CH2Cl2 (2 9 5 cm3) and then let evaporate in thefume hood. After evaporation were prepared samples forGC/MS by dissolving the solid or viscous liquid in pureCH2Cl2.
 

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