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Chemical Structure| 52083-08-6 Chemical Structure| 52083-08-6

Structure of 52083-08-6

Chemical Structure| 52083-08-6

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Product Details of [ 52083-08-6 ]

CAS No. :52083-08-6
Formula : C12H6O4
M.W : 214.17
SMILES Code : O=C(O1)C2=C3C(C1=O)=CC=CC3=C(O)C=C2
MDL No. :MFCD01013793
InChI Key :BFKXHILYGIQGCB-UHFFFAOYSA-N
Pubchem ID :5999497

Safety of [ 52083-08-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Application In Synthesis of [ 52083-08-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 52083-08-6 ]

[ 52083-08-6 ] Synthesis Path-Downstream   1~2

  • 1
  • aqueous fluoroboric acid [ No CAS ]
  • [ 6492-86-0 ]
  • [ 52083-08-6 ]
YieldReaction ConditionsOperation in experiment
With sodium nitrite; In sulfuric acid; water; EXAMPLE S3 4-Hydroxy-1,8-naphthalic anhydride To a solution of 1.0 g (4.7 mmol) of <strong>[6492-86-0]4-amino-1,8-naphthalic anhydride</strong> in 5 mL concentrated sulfuric acid at 0 C. to 5 C. was added 1.0 g (14.5 mmol) of sodium nitrite, and then 0.5 mL of water. The reaction was stirred for 30 minutes at 0 C. to 5 C., followed by addition of 5 mL (38 mmol) of 48% aqueous fluoroboric acid, with stirring for 30 minutes. The mixture was poured into ice water. The precipitate was isolated, suspended in a solution of 10 mL concentrated sulfuric acid in 50 mL water, refluxed in 3 hours, and again poured onto ice. The precipitate was isolated, washed with water, and dried to yield 620 mg of the title compound.
  • 2
  • [ 6492-86-0 ]
  • [ 52083-08-6 ]
 

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