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Chemical Structure| 50480-29-0 Chemical Structure| 50480-29-0

Structure of 50480-29-0

Chemical Structure| 50480-29-0

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Product Details of [ 50480-29-0 ]

CAS No. :50480-29-0
Formula : C7H7N3S
M.W : 165.22
SMILES Code : NC1=NC2=C(S1)C=CC(N)=C2
MDL No. :MFCD00781838
InChI Key :HGSZQBRMZNHXJZ-UHFFFAOYSA-N
Pubchem ID :768525

Safety of [ 50480-29-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 50480-29-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 50480-29-0 ]

[ 50480-29-0 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 73458-39-6 ]
  • [ 50480-29-0 ]
YieldReaction ConditionsOperation in experiment
66% With ethanol; tin(ll) chloride; at 80℃; for 4h; To a solution of ethanol (36 mL) was added [5-NITRO-BENZOTHIAZOL-2-YLAMINE] (Example 15,78 mg, [O 35 MMOL)] and tin dichloride dihydrate (449 [MG,] 2 [MMOL).] The resulting mixture was heated at [80C] for 4 hours. The solution was cooled to room temperature and the solvent was removed. The residue was dissolved in ethyl acetate and poured onto 50 mL of 1.5 N [NAOH] solution and extracted using ethyl acetate (3 x 30 mL). The combined organic layers were dried over [MGS04,] filtered and concentrated to give a solid (43 mg, [66%). 1H] NMR (DMSO d) 8 : 7.23-7. 19 (m, 3H), 6.59 (d, [1H,] J = 1.96 Hz), 6.32 (dd, [1 H,] J = 2.18, 8.28 Hz), 4.88 [(BR S,] 2H); MS [(ESI)] 166 [(M+1,] 100%).
 

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