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Chemical Structure| 4674-23-1 Chemical Structure| 4674-23-1

Structure of 4674-23-1

Chemical Structure| 4674-23-1

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Product Details of [ 4674-23-1 ]

CAS No. :4674-23-1
Formula : C20H26
M.W : 266.42
SMILES Code : CC1=C(CCC2=C(C)C=C(C)C=C2C)C(C)=CC(C)=C1

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Application In Synthesis of [ 4674-23-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 4674-23-1 ]

[ 4674-23-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 4761-00-6 ]
  • [ 4674-23-1 ]
YieldReaction ConditionsOperation in experiment
74% With {2,6-(Ph2PO)2-C6H3}NiCl; zinc; In N,N-dimethyl-formamide; at 115℃; for 16h;Inert atmosphere; General procedure: In a typical experiment, a mixture containing benzyl halide (1.0 mmol), nickel complex 1a (0.05 mmol) in DMF (5.0 mL) in a sealed tube was heated at 115 C under argon atmosphere for 16 h. To the cooled down solution was added water (20 mL), and then extracted with dichloromethane (10 mL×3). The combined organic layers were washed with of saturated NaClaq (20 mL) and dried over MgSO4. The crude product was purified by flash chromatography (4% EtOAc/hexanes) to afford the pure product.
  • 2
  • [ 4761-00-6 ]
  • [ 487-68-3 ]
  • [ 4170-90-5 ]
  • [ 4674-23-1 ]
 

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