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Chemical Structure| 41292-65-3 Chemical Structure| 41292-65-3
Chemical Structure| 41292-65-3

1H-Benzo[d]imidazol-5-ol

CAS No.: 41292-65-3

4.5 *For Research Use Only !

Cat. No.: A139233 Purity: 98%

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Product Details of [ 41292-65-3 ]

CAS No. :41292-65-3
Formula : C7H6N2O
M.W : 134.14
SMILES Code : OC1=CC=C2NC=NC2=C1
MDL No. :MFCD02241303
InChI Key :KRKSOBREFNTJJY-UHFFFAOYSA-N
Pubchem ID :3082533

Safety of [ 41292-65-3 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H332-H335
Precautionary Statements:P261-P280-P305+P351+P338

Application In Synthesis of [ 41292-65-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 41292-65-3 ]

[ 41292-65-3 ] Synthesis Path-Upstream   1~8

  • 1
  • [ 4887-80-3 ]
  • [ 41292-65-3 ]
YieldReaction ConditionsOperation in experiment
96% for 2 h; Heating / reflux Example 92; 4-(lH-Benzoimidazol-5-yloxy)-N-(4-bromo-phenyl)-3-(7-isopropyl-pyrido[2,3-d]pyrimidin-4- ylamino)-benzamide; Example 92A; lH-Benzoimidazol-5-ol; [0458] A solution of 5-methoxybenzimidazole (500 mg, 3.374 mmol) in 48percent hydrobromic acid (10 mL) was refluxed for 2 hours. The reaction was cooled to room temperature, the solvent removed by rotary evaporation under vacuum, and the residue azeotroped with toluene (50 mL) to provide the title compound as a tan solid (701 mg, 96percent).
References: [1] Patent: WO2007/76034, 2007, A2, . Location in patent: Page/Page column 125.
[2] Journal of the American Chemical Society, 1955, vol. 77, p. 5192.
[3] Synthetic Communications, 2010, vol. 40, # 12, p. 1765 - 1771.
[4] Bioorganic and Medicinal Chemistry Letters, 2012, vol. 22, # 7, p. 2620 - 2623.
  • 2
  • [ 610-81-1 ]
  • [ 122-51-0 ]
  • [ 41292-65-3 ]
References: [1] Heterocycles, 2008, vol. 75, # 8, p. 1907 - 1911.
  • 3
  • [ 64-18-6 ]
  • [ 610-81-1 ]
  • [ 41292-65-3 ]
References: [1] Tetrahedron Letters, 2005, vol. 46, # 39, p. 6741 - 6743.
[2] Synlett, 2010, # 18, p. 2759 - 2764.
  • 4
  • [ 106658-14-4 ]
  • [ 41292-65-3 ]
References: [1] Patent: US4704390, 1987, A, .
  • 5
  • [ 16133-49-6 ]
  • [ 41292-65-3 ]
References: [1] Bioorganic and Medicinal Chemistry Letters, 2012, vol. 22, # 7, p. 2620 - 2623.
  • 6
  • [ 102-51-2 ]
  • [ 41292-65-3 ]
References: [1] Bioorganic and Medicinal Chemistry Letters, 2012, vol. 22, # 7, p. 2620 - 2623.
  • 7
  • [ 50591-21-4 ]
  • [ 41292-65-3 ]
References: [1] Bulletin of the Chemical Society of Japan, 1958, vol. 31, p. 252.
  • 8
  • [ 25635-88-5 ]
  • [ 41292-65-3 ]
  • [ 4754-39-6 ]
References: [1] Journal of the American Chemical Society, 2015, vol. 137, # 33, p. 10444 - 10447.
 

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