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Chemical Structure| 41270-71-7 Chemical Structure| 41270-71-7

Structure of 41270-71-7

Chemical Structure| 41270-71-7

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Product Details of [ 41270-71-7 ]

CAS No. :41270-71-7
Formula : C16H13N3
M.W : 247.29
SMILES Code : NC1=NC(C2=CC=CC=C2)=C(C3=CC=CC=C3)N=C1

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Application In Synthesis of [ 41270-71-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 41270-71-7 ]

[ 41270-71-7 ] Synthesis Path-Downstream   1~1

  • 1
  • 2,3-diphenyloxirane [ No CAS ]
  • [ 69816-37-1 ]
  • [ 41270-71-7 ]
YieldReaction ConditionsOperation in experiment
87% With lithium bromide; In 1,4-dioxane; at 5 - 20℃; for 6h;Molecular sieve; Inert atmosphere; Reflux; Add 65mmol 2-aminoacetamidine hydrobromide, 2.5mmol lithium bromide, 7.5g molecular sieve and 100mL 1,4-dioxane into the reaction flask, stir at room temperature, fill with nitrogen, and reduce the temperature of the reaction system by 5-10C, and then Dissolve 50mmol of formula III compound in 50mL 1,4-dioxane and drop it into the above reaction flask. After dropping, stir and react at room temperature for 3h, then heat to reflux and keep the reaction at reflux for 3h, stop heating, and cool to After filtering at room temperature, the filtrate was distilled to dryness under reduced pressure, 150 mL of water was added, stirred for 0.5 h, the precipitated solid was filtered, the crude solid was recrystallized with ethanol, and dried under reduced pressure to obtain the compound of formula IV with a yield of 87%.
 

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