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Chemical Structure| 380380-59-6 Chemical Structure| 380380-59-6

Structure of 380380-59-6

Chemical Structure| 380380-59-6

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Product Details of [ 380380-59-6 ]

CAS No. :380380-59-6
Formula : C8H6BrN3O
M.W : 240.06
SMILES Code : CC1=NN=C(C2=NC=CC(Br)=C2)O1
MDL No. :MFCD16658665

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Application In Synthesis of [ 380380-59-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 380380-59-6 ]

[ 380380-59-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 380380-60-9 ]
  • [ 380380-59-6 ]
YieldReaction ConditionsOperation in experiment
75% Intermediate 37 (5.3 g, 23.4 mol) was dissolved in Ac2O (80 mL) at r.t. and pyridine (9.2 mL) was added. The mixture was heated to 130 C. for 1.5 h. Then the solution was poured into ice-water (400 mL) and PH was adjusted to 3-4 with 6 N HCl (aq). The mixture was stirred for 20 min and filtered. The desired product was collected as a white solid (4.25 g, 75%).
 

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