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Chemical Structure| 379228-27-0 Chemical Structure| 379228-27-0

Structure of 379228-27-0

Chemical Structure| 379228-27-0

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Product Details of [ 379228-27-0 ]

CAS No. :379228-27-0
Formula : C10H10N2O3
M.W : 206.20
SMILES Code : O=C1NC=NC2=C1C(OC)=CC(OC)=C2
MDL No. :MFCD13191849
InChI Key :AMCMSZVLSWCVQX-UHFFFAOYSA-N
Pubchem ID :135510667

Safety of [ 379228-27-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 379228-27-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 379228-27-0 ]

[ 379228-27-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 3473-63-0 ]
  • [ 379228-26-9 ]
  • [ 379228-27-0 ]
YieldReaction ConditionsOperation in experiment
In 2-methoxy-ethanol; A mixture of <strong>[379228-26-9]methyl 2-amino-4,6-dimethoxybenzoate</strong> (16 g), formamidine acetate (24 g) and 2-methoxyethanol (330 ml) was stirred and heated to reflux until all of the starting material had reacted. The mixture was evaporated and the residue was triturated under water (100 ml). The resultant solid was isolated, washed with water and dried under vacuum to give 5,7-dimethoxy-3,4-dihydroquinazolin-4-one (14.5 g); NMR Spectrum : (DMSOd6) 3.82 (s, 3H), 3.86 (s, 3H), 6.5 (s, 1H), 6.7 (s, 1H), 7.9 (s, 1H), 11.7 (br s, 1H).
 

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