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Chemical Structure| 37441-29-5 Chemical Structure| 37441-29-5

Structure of 37441-29-5

Chemical Structure| 37441-29-5

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Product Details of [ 37441-29-5 ]

CAS No. :37441-29-5
Formula : C8H2Cl2I3NO2
M.W : 595.73
SMILES Code : ClC(C1=C(C(C(Cl)=O)=C(C(N)=C1I)I)I)=O
MDL No. :MFCD00270836
InChI Key :FBJVWRITWDYUAC-UHFFFAOYSA-N
Pubchem ID :9894858

Safety of [ 37441-29-5 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P301+P330+P331-P303+P361+P353-P363-P304+P340-P310-P321-P260-P264-P280-P305+P351+P338-P405-P501
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 37441-29-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 37441-29-5 ]

[ 37441-29-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 35453-19-1 ]
  • [ 37091-73-9 ]
  • 5-amino-2,4,6-triodoisophthaloyl dichloride [ No CAS ]
  • [ 37441-29-5 ]
YieldReaction ConditionsOperation in experiment
95% In hexane; toluene; Example 7 Synthesis of 5-amino-2,4,6-triodoisophthaloyl dichloride To a reaction flask, 4.23 g (0.025 mole) of <strong>[37091-73-9]2-chloro-1,3-dimethylimidazolinium chloride</strong>, 5.58 g (0.01 mole) of 5-amino-2,4,6-triiodoisophthalic acid and 80 g of toluene were charged and reacted at 105°-110° C. for 4 hours. Thereafter, the reaction mass was cooled and toluene was removed under reduced pressure. To the concentrate thus obtained, 100 ml of hexane was added to crystallize 5-amino-2,4,6-triiodoisophthaloyl dichloride. The precipitate was filtered and dried under reduced pressure to obtain 5.65 g (95percent yield) of 5-amino-2,4,6-triiodoisophthaloyl dichloride as white crystals.
  • 2
  • [ 35453-19-1 ]
  • [ 37091-73-9 ]
  • [ 37441-29-5 ]
YieldReaction ConditionsOperation in experiment
93% Example 8 Synthesis of 5-amino-2,4,6-triodoisophthaloyl dichloride The same procedures as described in Example 7 were carried out except that the reaction of 5-amino-2,4,6-triiodoisophthalic acid and <strong>[37091-73-9]2-chloro-1,3-dimethylimidazolinium chloride</strong> was carried out at 90°-95° C. for 6 hours. 5-Amino-2,4,6-triiodoisophthaloyl dichloride thus obtained was 5.53 g (93percent yield).
 

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