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Chemical Structure| 29067-55-8 Chemical Structure| 29067-55-8

Structure of 29067-55-8

Chemical Structure| 29067-55-8

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Product Details of [ 29067-55-8 ]

CAS No. :29067-55-8
Formula : C8H8BrNO2
M.W : 230.06
SMILES Code : O=[N+](C1=CC(C(Br)C)=CC=C1)[O-]

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Application In Synthesis of [ 29067-55-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 29067-55-8 ]

[ 29067-55-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 5400-78-2 ]
  • [ 29067-55-8 ]
YieldReaction ConditionsOperation in experiment
With hydrogen bromide; acetic acid; In water; at 20℃; for 120h;Cooling with ice; Step bPreparation of 1-(1-bromoethyl)-3-nitrobenzene26.15 g (156 mmol) of <strong>[5400-78-2]1-(3-nitrophenyl)ethanol</strong> are dissolved in 130 ml of glacial acetic acid, and 55 ml (313 mmol) of 33% HBr in glacial acetic acid are added dropwise with ice cooling. The reaction mixture is stirred at room temperature for 5 days. The mixture is subsequently diluted with 300 ml of DCM, washed with 3×200 ml of H2O and 200 ml of saturated NaHCO3 solution, dried over sodium sulfate and evaporated to dryness, and the residue is crystallised from petroleum ether.Product: 30.4 g; HPLC: Rt=5.39 min (method A).
 

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