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Chemical Structure| 29067-53-6 Chemical Structure| 29067-53-6

Structure of 29067-53-6

Chemical Structure| 29067-53-6

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Product Details of [ 29067-53-6 ]

CAS No. :29067-53-6
Formula : C9H11NO3
M.W : 181.19
SMILES Code : CCC(C1=CC=CC([N+]([O-])=O)=C1)O
MDL No. :MFCD11867370

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Application In Synthesis of [ 29067-53-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 29067-53-6 ]

[ 29067-53-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 17408-16-1 ]
  • [ 29067-53-6 ]
YieldReaction ConditionsOperation in experiment
With methanol; sodium tetrahydroborate; at 0 - 20℃; for 1h; Example 11 : Preparation of compound 1045Step 1 :<strong>[17408-16-1]3-Nitropropiophenone</strong> (300 mg, 1.67 mmol, Aldrich) is dissolved in MeOH (16 mL) and cooled to 0C. Sodium borohydride (76 mg, 2.00 mmol) is added and the reaction mixture is stirred for 1 h at RT. The reaction mixture is concentrated under vacuum to dryness. The crude material is purified by flash chromatography (25% EtOAc in Hex to 35% EtOAc in Hex) to isolate product 11.1.
 

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