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Chemical Structure| 245762-35-0 Chemical Structure| 245762-35-0

Structure of 245762-35-0

Chemical Structure| 245762-35-0

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Product Details of [ 245762-35-0 ]

CAS No. :245762-35-0
Formula : C8H7FO
M.W : 138.14
SMILES Code : FC1=CC=C2OCCC2=C1
MDL No. :MFCD08236758
InChI Key :PAVTXINZFWRQOD-UHFFFAOYSA-N
Pubchem ID :22398640

Safety of [ 245762-35-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H312-H332
Precautionary Statements:P280

Application In Synthesis of [ 245762-35-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 245762-35-0 ]

[ 245762-35-0 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 24410-59-1 ]
  • [ 245762-35-0 ]
YieldReaction ConditionsOperation in experiment
85% With hydrogen;palladium 10% on activated carbon; In acetic acid; under 2585.81 Torr; for 12h; A solution of <strong>[24410-59-1]5-fluorobenzofuran</strong> and 10% palladium on carbon in acetic acid (25 ml) was hydrogenated under 50 psi for 12 hours. The catalyst was filtered through celite and the celite was washed with methylene chloride (200 ml). The organic layer was washed sequentially with 1N NaOH (3 x 100 ml), brine (3 x 100 ml) and dried over anhydrous sodium sulfate and filtered. The solvent was removed under vacuum to afforded 2.59 g (85%) of product as a clear oil: 1H NMR (300 MHz, CDCl3): delta 3.12 (t, 2H, J = 8.7 Hz), 4.58 (t, 2H, J = 8.7 Hz), 6.68 (dd, 1H, J = 8.7, 4.2 Hz), 6.79 (tm, 1H, J = 8.7 Hz), 6.89 (dm, 1H, J = 8.1 Hz).
  • 3
  • [ 17403-47-3 ]
  • [ 245762-35-0 ]
 

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