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[ CAS No. 2314-78-5 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 2314-78-5
Chemical Structure| 2314-78-5
Structure of 2314-78-5 * Storage: {[proInfo.prStorage]}
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Product Details of [ 2314-78-5 ]

CAS No. :2314-78-5 MDL No. :MFCD00059748
Formula : C6H9NO2 Boiling Point : -
Linear Structure Formula :- InChI Key :GHAZCVNUKKZTLG-UHFFFAOYSA-N
M.W : 127.14 Pubchem ID :16842
Synonyms :

Safety of [ 2314-78-5 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313 UN#:N/A
Hazard Statements:H315-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 2314-78-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2314-78-5 ]

[ 2314-78-5 ] Synthesis Path-Downstream   1~12

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YieldReaction ConditionsOperation in experiment
With dihydrogen peroxide In water at 160℃; for 120h; Autoclave; The gas chromatography-mass spectroscopy (GC-MS) spectrumindicated that there were no detectable organic compoundsin the starting purified triethylamine. In a typical synthesis,0.6 ml (4.3 mmol) purified triethylamine and 10 mL 30% (0.1 mol)hydrogen peroxide solution were mixed with water and then added into each steel alloy (Fe-Cr-Ni alloy, GB-1220-92) autoclavewith a filling capacity of 90% (approx. 1.4 MPa). The autoclaveswere then sealed tightly and placed in the oven with the temperatureranging from 20 to 200 C at the interval of every 20 C. After5 days, the solution in the autoclaves was taken out and analyzed.The final pH of the reaction mixture was 9.7. Gas chromatography-mass spectroscopy (GC-MS) was employed to identify theproducts. It is proved that 120 C is a turning point: when the temperatureis lower than that, the main product is N,N-diethylhydroxylamine(1); on the contrary, the product is more complex andthe main products are amides: N,N-diethylacetamide(2),N-ethylacetamide(3), acetylamine(4), and 1-ethylpyrrolidine-2,5-dione(5), when the mass spectra of the products were comparedto those of standard substances (Figs. S1-S5). The reaction can berepresented as follows:
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YieldReaction ConditionsOperation in experiment
1: 67.9 %Chromat. 2: 8.7 %Chromat. With carbon dioxide at 150℃; for 18h; Green chemistry;
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  • [ 16078-30-1 ]
  • 3-(1-acetylindolin-7-yl)-1-ethylpyrrolidine-2,5-dione [ No CAS ]
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