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Chemical Structure| 22936-83-0 Chemical Structure| 22936-83-0

Structure of 22936-83-0

Chemical Structure| 22936-83-0

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Product Details of [ 22936-83-0 ]

CAS No. :22936-83-0
Formula : C4H9N
M.W : 71.12
SMILES Code : NC1(C)CC1
MDL No. :MFCD11109576

Safety of [ 22936-83-0 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H225-H314
Precautionary Statements:P210-P280-P305+P351+P338-P310
Class:3(8)
UN#:2924
Packing Group:

Application In Synthesis of [ 22936-83-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 22936-83-0 ]

[ 22936-83-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 15910-91-5 ]
  • [ 22936-83-0 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; bromine; In water; at 0 - 80℃; for 28.5h; Bromine (2. 87mol, 0. 056mol) was added to a solution of sodium hydroxide (13. 5g, 0. 338mol) in water (100ml) at 0-5 C. A slurry of 1- (1-methylcyclopropane) carboxamide (Method 51 ; 5.70g 0. 056mol) in water (sol) was then added and reaction mixture stirred at 5 C for 2 hours, then left to stand at ambient temperature for 24 hours. The mixture was then heated at 80 C for 2.5 hours, allowed to cool and mixture distilled to give the title compound (bp 75-80 C). NMR : 0.2 (q, 2H), 0.14 (q, 2H), 0.96 (s, 3H), 1.42 (s, 2H).
 

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