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[ CAS No. 214774-61-5 ] 2,4-Dichloro-1-fluoro-3,5-dimethylbenzene

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CAS No. :214774-61-5 MDL No. :MFCD04972785
Formula : C8H7Cl2F Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 193.05 Pubchem ID :-
Synonyms :

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 214774-61-5 ]

[ 214774-61-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 461-97-2 ]
  • [ 214774-61-5 ]
YieldReaction ConditionsOperation in experiment
With iron(III) chloride; In chlorine; 1,2-dichloro-ethane; b) in 1,2-dichloroethane 1 kg of <strong>[461-97-2]3,5-dimethyl-fluorobenzene</strong> and 15 g of anhydrous iron(III) chloride are introduced into 11 of 1,2-dichloroethane and chlorine is passed in at the rate at which the reaction proceeds (about 4 h). The reaction is initially exothermic (temperature rise from 24 to 32° C.) and is kept below 30° C. by cooling. After passing in 1200 g of chlorine, 4percent of monochloro compound, 81.1percent of desired product and 13.3percent of overchlorinated compounds are formed according to GC analysis.
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