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Chemical Structure| 21022-17-3 Chemical Structure| 21022-17-3

Structure of 21022-17-3

Chemical Structure| 21022-17-3

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Product Details of [ 21022-17-3 ]

CAS No. :21022-17-3
Formula : C26H20N2O2
M.W : 392.45
SMILES Code : O=C(NC1=CC=CC=C1C2=CC=CC=C2)C(NC3=CC=CC=C3C4=CC=CC=C4)=O
MDL No. :MFCD31793560
InChI Key :VKRWRNVGVPSVLA-UHFFFAOYSA-N
Pubchem ID :333906

Safety of [ 21022-17-3 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H319-H372-H410
Precautionary Statements:P260-P264-P273-P301+P312-P305+P351+P338-P314
Class:9
UN#:3077
Packing Group:

Application In Synthesis of [ 21022-17-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 21022-17-3 ]

[ 21022-17-3 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 90-41-5 ]
  • [ 95-92-1 ]
  • [ 24451-19-2 ]
  • [ 21022-17-3 ]
  • 2
  • [ 90-41-5 ]
  • [ 95-92-1 ]
  • [ 21022-17-3 ]
  • 3
  • [ 116490-13-2 ]
  • trichlorophosphate [ No CAS ]
  • [ 1015-89-0 ]
  • [ 21022-17-3 ]
  • 5
  • C7H4INO4 [ No CAS ]
  • [ 3128-77-6 ]
  • [ 21022-17-3 ]
YieldReaction ConditionsOperation in experiment
64% With copper(l) iodide; In 1,4-dioxane; at 80℃; for 2.0h; Will be 0.5mmol2-phenylbenzene isonitrile (89.5 mg),(219.8 mg), 0.1 mmol of cuprous iodide (19.1 mg) and 5 mL of 1,4-dioxane were added to a 15 mL reaction tube. Subsequently, the mixture was magnetically stirred at 80 C for 2 hours. Then, two syrups of silica gel (100-200 mesh) were added to the reaction solution, and the solvent was removed by distillation under reduced pressure. The residue was packed in column and separated by column chromatography using petroleum ether, 10: 1 as the eluent, the eluate containing the product was collected and the solvent was distilled off to give the pure product 2,2'-diphenyl oxalanilide. The material was a pale yellow solid in 64% yield.
  • 6
  • [ 90-41-5 ]
  • [ 127563-31-9 ]
  • [ 21022-17-3 ]
  • 7
  • [ 90-41-5 ]
  • [ 21022-17-3 ]
 

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