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Chemical Structure| 20358-05-8

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Product Details of [ 20358-05-8 ]

CAS No. :20358-05-8
Formula : C7H5BrN2S
M.W : 229.10
SMILES Code : NC1=NC2=CC=CC(Br)=C2S1
MDL No. :MFCD11110957
InChI Key :YHKASBDRJLTLHH-UHFFFAOYSA-N
Pubchem ID :20357112

Safety of [ 20358-05-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 20358-05-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 20358-05-8 ]

[ 20358-05-8 ] Synthesis Path-Downstream   1~2

  • 1
  • C14H10BrN2OPolS [ No CAS ]
  • [ 20358-03-6 ]
  • [ 20358-05-8 ]
  • 2
  • [ 21327-14-0 ]
  • [ 20358-03-6 ]
  • [ 20358-05-8 ]
YieldReaction ConditionsOperation in experiment
With bromine; In dichloromethane; at 20℃; [838] Step 1: a mixture of 5-bromobenzo[d]thiazol-2-amine and 7-bromobenzo[d]thiazol-2-amine[839] To a stirred solution of 1-(3-bromophenyl)thiourea (1.00 g, 4.33 mmol) in dichloromethane (15 mL) was added dropwise a solution of bromine (345 mg, 4.33 mmol) in dichloromethane (15 mL). The reaction mixture was stirred at room temperature overnight. The resulting solid was filtered, washed with dichloromethane, and then dried under reduced pressure to give 809 mg of the titled compound as a yellow solid (Yield: 82percent).
With bromine; In dichloromethane; at 20℃; Step 1: a mixture of 5-bromobenzo[d]thiazol-2-amine and 7-bromobenzo[d]thiazol-2-amine [0484] To a stirred solution of 1-(3-bromophenyl)thiourea (1.00 g, 4.33 mmol) in dichloromethane (15 mL) was added dropwise a solution of bromine (345 mg, 4.33 mmol) in dichloromethane (15 mL). The reaction mixture was stirred at room temperature overnight. The resulting solid was filtered, washed with dichloromethane, and then dried under reduced pressure to give 809 mg of the titled compound as a yellow solid (Yield: 82percent).
 

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Technical Information

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Related Functional Groups of
[ 20358-05-8 ]

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Related Parent Nucleus of
[ 20358-05-8 ]

Benzothiazoles

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