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Chemical Structure| 203180-01-2 Chemical Structure| 203180-01-2

Structure of 203180-01-2

Chemical Structure| 203180-01-2

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Product Details of [ 203180-01-2 ]

CAS No. :203180-01-2
Formula : C6H6IN5O
M.W : 291.05
SMILES Code : NC1=NC(OC)=C2C(NN=C2I)=N1

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Application In Synthesis of [ 203180-01-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 203180-01-2 ]

[ 203180-01-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 100644-67-5 ]
  • [ 203180-01-2 ]
YieldReaction ConditionsOperation in experiment
78.8% With sodium acetate; Iodine monochloride; In water; at 95℃; for 2.5h;Darkness; Inert atmosphere; Sodium acetate and the formula (V) compound (675mg, 4.09mmol) (1.73g, 21.08mmol) was added 15mL of water, under dark, adding iodine chloride (905mg, 5.58mmol), nitrogen, 95 C under reflux for 2.5h After adding 20mL of water and sodium metabisulfite (1.1g, 5.79mmol), stirred at room temperature for 0.5h filtered in vacuo Dried to give a pale red solid 938mg, yield 78.8%.
 

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