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Chemical Structure| 201006-49-7 Chemical Structure| 201006-49-7

Structure of 201006-49-7

Chemical Structure| 201006-49-7

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Product Details of [ 201006-49-7 ]

CAS No. :201006-49-7
Formula : C6H6ClNS
M.W : 159.63
SMILES Code : ClC1=NC2=C(CCC2)S1
MDL No. :MFCD17249938

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Application In Synthesis of [ 201006-49-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 201006-49-7 ]

[ 201006-49-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 53051-97-1 ]
  • [ 201006-49-7 ]
YieldReaction ConditionsOperation in experiment
With tert.-butylnitrite; copper(l) chloride; In acetonitrile; at 20 - 65℃; for 3h; 2-Amino-5,6-dihydro-4H-cyclopentathiazole (230 mg, 1.64 mmol) was added to a solution of cupric chloride (260 mg, 1.97 mmol) and ferf-butylnitrite (0.3 ml, 2.46 mmol) in MeCN (0.5 ml) and the resulting mixture was stirred for 2 h at room temperature, then at 650C for 1 h. The reaction was filtered and the filtrate partitioned between water and EtOAc. The organic fraction was dried (MgSO4), filtered and concentrated under reduced pressure to give the chloride (140 mg), which was used without further purification. MS: [M+H]+ = 160.
 

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