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Chemical Structure| 197313-74-9 Chemical Structure| 197313-74-9

Structure of 197313-74-9

Chemical Structure| 197313-74-9

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2,3-Diphenyl-1H-indole-7-carboxylic acid

CAS No.: 197313-74-9

,97%

4.5 *For Research Use Only !

Cat. No.: A312748 Purity: 97%

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    Product Details of [ 197313-74-9 ]

    CAS No. :197313-74-9
    Formula : C21H15NO2
    M.W : 313.35
    SMILES Code : O=C(C1=CC=CC2=C1NC(C3=CC=CC=C3)=C2C4=CC=CC=C4)O
    MDL No. :MFCD00572872

    Safety of [ 197313-74-9 ]

    Application In Synthesis of [ 197313-74-9 ]

    * All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

    • Downstream synthetic route of [ 197313-74-9 ]

    [ 197313-74-9 ] Synthesis Path-Downstream   1~2

    • 1
    • [ 119-53-9 ]
    • [ 118-92-3 ]
    • anthranilic acid-hydrochloride [ No CAS ]
    • [ 3469-20-3 ]
    • [ 197313-74-9 ]
    • 2
    • [ 451-40-1 ]
    • [ 33906-30-8 ]
    • [ 197313-74-9 ]
    YieldReaction ConditionsOperation in experiment
    24% <strong>[33906-30-8]2-hydrazinobenzoic acid hydrochloride</strong> (5.00 g, 30.08 mmol) and deoxybenzoin (5.90 g, 30.08 mmol) was refluxed in ACOH (100 ml) for 30 min, cone. HCI (50 ml) was added and mixture refluxed for 4 h. Water (800 ml) was added and a white solid precipitated. The solid was filtered, washed with water and recryst. from EtOAc (100 ml). Yield 2.23 g (24%); white solid. Mp. 262 C. 'H NMR (400 MHz, DMSO-d6) 6 7. 18 (t, J=8 Hz, 1 H), 7.27-7. 47 (M, 10 H), 7.75 (d, J=8 Hz, 1 H), 7.82 (d, J=8 Hz, 1 H), 10.73 (s, 1 H), 13.19 (s, 1 H). 13C NMR (100 MHz, DMSO-d6) 8 113. 80,113. 99,119. 68,124. 08,124. 72,126. 47,127. 97,128. 48,128. 72, 129.36, 129.86, 131.69, 134.35, 135.05, 135.38, 167.94. Found: 313.1117 (M). Calc. for C2LHL5NO2 : 313.1103. CAS [197313-74-9].
     

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