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Chemical Structure| 18714-17-5 Chemical Structure| 18714-17-5

Structure of 18714-17-5

Chemical Structure| 18714-17-5

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Product Details of [ 18714-17-5 ]

CAS No. :18714-17-5
Formula : C13H11NO2
M.W : 213.23
SMILES Code : O=C(OC)C1=NC=CC(C2=CC=CC=C2)=C1
MDL No. :MFCD13181692

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Application In Synthesis of [ 18714-17-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 18714-17-5 ]

[ 18714-17-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 67-56-1 ]
  • [ 42260-39-9 ]
  • [ 201230-82-2 ]
  • [ 18714-17-5 ]
YieldReaction ConditionsOperation in experiment
71% With triethylamine;(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; at 70℃; under 30003.0 Torr; To a solution of 2 (2 g, 0.01 mol) in MeOH (100 mL) were added TEA (5.33 g, 0.05 mol) andPdCl2(dppf) (0.5 g). The reaction mixture was stirred overnight at 70 °C under 4 MPa CO. The suspension was filtered through a pad of celite and washed with MeOH. The combined filtrates were concentrated in vacuo. Purification on silica gel (PE: E A=I 0: 1) afforded 1.5 g of 3 (yield71percent).
 

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