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Chemical Structure| 181376-12-5 Chemical Structure| 181376-12-5

Structure of 181376-12-5

Chemical Structure| 181376-12-5

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Product Details of [ 181376-12-5 ]

CAS No. :181376-12-5
Formula : C7H5IN2O3
M.W : 292.03
SMILES Code : O=C(N)C1=CC([N+]([O-])=O)=CC=C1I

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Application In Synthesis of [ 181376-12-5 ]

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  • Downstream synthetic route of [ 181376-12-5 ]

[ 181376-12-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 19230-50-3 ]
  • [ 181376-12-5 ]
YieldReaction ConditionsOperation in experiment
I. 2-Iodo-5-Nitro-Benzamide 2-iodo-5-nitro-benzamide was synthesised by the method previously described for 4-iodo-5-nitro-benzamide using <strong>[19230-50-3]2-iodo-5-nitro benzoic acid</strong> (Chemica Alta Ltd., Edmonton, Alberta, Canada) as the starting material. 1 H NMR Spectrum, in DMSO-d6 delta (ppm) values relative to TMS: 7.742 (1H, singlet); 7.943 (1H, doublet of doublts, J=8.26 Hz, J=2.58 Hz); 8.034 (1H, singlet), 8.064 (1H, doublet, J=2.94 Hz); and 8.191 (1H, doublet, J=8.46 Hz). Mass Spectrum: Low resolution electron impact spectrum (m/z): 292 (M+), 276, 230, 202, 165, 127, 91, 75, 63. High resolution measurement of M+: Calculated for C7 H5 IN2 O3: 291.934494; found: 291.934149 (deviation=1.2 ppm).
 

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