Home Cart Sign in  
Chemical Structure| 1776-56-3 Chemical Structure| 1776-56-3

Structure of 1776-56-3

Chemical Structure| 1776-56-3

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1776-56-3 ]

CAS No. :1776-56-3
Formula : C12H15NO3
M.W : 221.25
SMILES Code : O=C(C1=CC=CC=C1)NCC(OC(C)C)=O
MDL No. :MFCD23144592

Safety of [ 1776-56-3 ]

Application In Synthesis of [ 1776-56-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1776-56-3 ]

[ 1776-56-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 14019-62-6 ]
  • [ 98-88-4 ]
  • [ 1776-56-3 ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In chloroform; at 0 - 60℃; for 7h; General procedure: A solution of L-ethyl glycinate hydrochloride and sorbic chloride in chloroform (15ml) was added to triethylamine (2ml, 0.014mol) with stirring at 0C for 3h and then at 60C for 4h. The reaction mixture was poured into water (25ml), extracted with ethyl acetate (3×25ml), washed with NaOH solution (0.5mol/l, 2×25ml) and then dried over anhydrous MgSO4. After removal of the solvent under reduced pressure, the residual paste was purified by column chromatography (silica gel, petroleum ether/ethyl acetate, 2:1) to give Etheyl N-[1-oxo-2, 4-hexadien-1-yl] glycinate (a1). Other compounds (a2-a7 and b1-b7) were synthesized using procedures similar to that described above for compound a1.
 

Historical Records

Technical Information

Categories