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Chemical Structure| 17653-94-0 Chemical Structure| 17653-94-0

Structure of 17653-94-0

Chemical Structure| 17653-94-0

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Product Details of [ 17653-94-0 ]

CAS No. :17653-94-0
Formula : C11H14O3
M.W : 194.23
SMILES Code : COC1=CC=CC(=C1)C(C)(C)C(O)=O
MDL No. :MFCD09414710
InChI Key :AJBGTOYTKPVUPX-UHFFFAOYSA-N
Pubchem ID :10821634

Safety of [ 17653-94-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 17653-94-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17653-94-0 ]

[ 17653-94-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 32454-33-4 ]
  • [ 17653-94-0 ]
YieldReaction ConditionsOperation in experiment
To <strong>[32454-33-4]methyl 2-(3-methoxyphenyl)-2-methylpropanoate</strong> (800mg, 4 mmol) in THF (10 ml) and MeOH (10 ml), aqueous LiOH (excess) was added and the reaction mixture was heated at 6O0C for 7h. Then volatiles were removed in vacuum and the aqueous layer was extracted with ether. Ether layer was discarded. Then the aqueous layer was acidified and extracted with ethyl acetate. Organic layer was dried with sodium sulfate and volatiles removed under vacuum to yield 2-(3-methoxyphenyl)-2-methylpropanoic acid.
 

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