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Chemical Structure| 174138-01-3 Chemical Structure| 174138-01-3

Structure of 174138-01-3

Chemical Structure| 174138-01-3

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Product Details of [ 174138-01-3 ]

CAS No. :174138-01-3
Formula : C16H31N3O4
M.W : 329.44
SMILES Code : O=C(N1CCN(C(OC(C)(C)C)=O)CCNCC1)OC(C)(C)C
MDL No. :MFCD30532166

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Application In Synthesis of [ 174138-01-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 174138-01-3 ]

[ 174138-01-3 ] Synthesis Path-Downstream   1~2

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  • [ 58966-93-1 ]
  • [ 174138-01-3 ]
  • 2
  • [ 58632-95-4 ]
  • [ 58966-93-1 ]
  • [ 174138-01-3 ]
YieldReaction ConditionsOperation in experiment
100% With N-ethyl-N,N-diisopropylamine; In chloroform; for 120h; To a solution of 1,4,7-triazonane trihydrogenchloride (TACN 3HC1, 1.85 g, 7.7 mmol, M.W.:238.6) in CHCl3 (25 mL) was added DIPEA (4.0 mL, 3.0 g, 23.1 mmol, M.W.: 129.24, d: 0.742) and BOC-ON (3.77 g, 15.3 mmol, M.W.: 246.26) in portions. The resulting mixture was stirred for 5 days and the solvent evaporated under vacuum. The residue was partitioned between 10% NaOH solution (10 mL) and diethyl ether (30 mL). The ether layer was separated and washed with 10% NaOH solution (10 mL) and water (10 mL) several times. The ether layer was dried (MgS04), filtered, and concentrated under vacuum to provide QC04001 (2.53 g, quantitative), which was used without furher purification.
 

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