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Chemical Structure| 173157-33-0 Chemical Structure| 173157-33-0

Structure of 173157-33-0

Chemical Structure| 173157-33-0

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Product Details of [ 173157-33-0 ]

CAS No. :173157-33-0
Formula : C7H6INO2
M.W : 263.03
SMILES Code : O=C(OC)C1=CN=C(I)C=C1
MDL No. :MFCD12546492
InChI Key :CGFVEUUNDFAFHE-UHFFFAOYSA-N
Pubchem ID :14784670

Safety of [ 173157-33-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 173157-33-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 173157-33-0 ]

[ 173157-33-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 13054-02-9 ]
  • [ 18107-18-1 ]
  • [ 173157-33-0 ]
YieldReaction ConditionsOperation in experiment
In methanol; toluene; at 0 - 20℃; for 2.0h; 6-Iodo-nicotinic acid methyl ester To a mixture of 6-Iodo-nicotinic acid (6.8 g, 27.4 mmol), toluene (40 mL) and MeOH (40 mL) cooled at 0 C, was added TMS diazomethane dropwise. The reaction mixture was then stirred at ambient temperature for additional 2 hours. The reaction mixture was concentrated in vacuo, the yellow residue was recrystallized from toluene to give the desired product as yellow crystals (5.6 g), MP 136-138 C, MS (APCI+) : n2/z 263.8 (M+H).
 

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[ 173157-33-0 ]

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