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Chemical Structure| 17285-37-9 Chemical Structure| 17285-37-9

Structure of 17285-37-9

Chemical Structure| 17285-37-9

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Product Details of [ 17285-37-9 ]

CAS No. :17285-37-9
Formula : C4H2Cl2N2O
M.W : 164.98
SMILES Code : ClC1=NNC(=O)C(Cl)=C1
MDL No. :MFCD21099563
InChI Key :WUEIRRXSGRRWKG-UHFFFAOYSA-N
Pubchem ID :58016205

Safety of [ 17285-37-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H332-H335
Precautionary Statements:P280-P305+P351+P338-P310

Application In Synthesis of [ 17285-37-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17285-37-9 ]

[ 17285-37-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 6082-66-2 ]
  • [ 64-19-7 ]
  • [ 17285-37-9 ]
  • [ 17285-36-8 ]
  • 2
  • [ 6082-66-2 ]
  • [ 17285-37-9 ]
  • [ 17285-36-8 ]
YieldReaction ConditionsOperation in experiment
With acetic acid; at 100.0℃; for 12.0h; A solution of 3,4,6-trichloropyridazine (20.0 g, 109.04 mmol) in HOAc (100 mL) was heated at 100 °C for 12 h, at which time TLC indicated the reaction had gone to completion. The reaction mixture was concentrated under reduced pressure, and the resulting residue was purified by silica gel chromatography (petroleum ether : Ethyl acetate = 1 : 1 ) to give the title compounds (11.2 g, 63percent yield) (1 : 1 ratio of regioisomers) as a white solid. LCMS M/Z (M+H) 165.
 

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