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Chemical Structure| 1705-89-1 Chemical Structure| 1705-89-1
Chemical Structure| 1705-89-1
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Product Details of [ 1705-89-1 ]

CAS No. :1705-89-1
Formula : C14H10O
M.W : 194.23
SMILES Code : O=C1C2=C(C3=C1C=CC=C3)C=C(C)C=C2
MDL No. :MFCD00453961

Safety of [ 1705-89-1 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H318-H411
Precautionary Statements:P280-P305+P351+P338+P310
Class:9
UN#:3077
Packing Group:

Application In Synthesis of [ 1705-89-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1705-89-1 ]

[ 1705-89-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 26260-02-6 ]
  • [ 262373-15-9 ]
  • [ 2840-51-9 ]
  • [ 1705-89-1 ]
  • 2
  • 2-(4-methylbenzoyl)benzenediazonium tetrafluoroborate [ No CAS ]
  • [ 174899-66-2 ]
  • [ 1705-89-1 ]
  • C15H11F3O4S [ No CAS ]
YieldReaction ConditionsOperation in experiment
at 80℃; for 1.5h; General procedure: The diazonium tetrafluoroborates (10-20 mg) were dissolved in ionic liquids (0.4 mL). The solution was heated using the conditions shown in Table 1. The ionic liquids were extracted with hexane. After removal of the solvent, the residues were analyzed by NMR, and the product distributions are summarized in Table 1. Compounds 2a,22 2b,23 2c,24 2d,23 2e,22 3a,25 3d,26 3e,27 and 3f27 were identified by comparing their NMR spectra with those reported in the literature. The isomers ArOSO(CF3)(NTf) (4a-4f) and ArNTf2 (5a-5f) were attempted to be purified with SiO2 column chromatography using hexane-CH2Cl2 or hexane-ether as an eluent. However, they could not be separated by chromatography.
 

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