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Chemical Structure| 1657-50-7 Chemical Structure| 1657-50-7

Structure of 1657-50-7

Chemical Structure| 1657-50-7

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Product Details of [ 1657-50-7 ]

CAS No. :1657-50-7
Formula : C14H11Cl
M.W : 214.69
SMILES Code : ClC1=CC=C(/C=C/C2=CC=CC=C2)C=C1

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Application In Synthesis of [ 1657-50-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1657-50-7 ]

[ 1657-50-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 100-42-5 ]
  • [ 14752-66-0 ]
  • [ 1657-50-7 ]
YieldReaction ConditionsOperation in experiment
72% With ammonium hexafluorophosphate; 4,4′,5,5′-Tetrahydro-2,2′-bioxazole; acetic acid; palladium dichloride; In water; N,N-dimethyl-formamide; at 60℃; for 18h; General procedure: To a mixture of PdCl2 (5.3 mg, 0.03 mmol), 2,2’-bis(2-oxazoline) (4.6 mg, 0.033 mmol), and PhSO2Na(59.5 mg, 0.33 mmol) and NH4PF6 (14.7 mg, 0.09 mmol) in DMF (0.3 mL), H2O (0.2 mL) and AcOH(0.1 mL) were added styrene (31.2 mg, 0.3 mmol), and the mixture was stirred at 60 C for 18 h in air.After the residue was dissolved in Et2O, the solution was washed with H2O and saturated sodiumchloride and dried over anhydrous magnesium sulfate
 

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