Home Cart Sign in  
Chemical Structure| 161490-19-3 Chemical Structure| 161490-19-3

Structure of 161490-19-3

Chemical Structure| 161490-19-3

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 161490-19-3 ]

CAS No. :161490-19-3
Formula : C8H19N3O2
M.W : 189.26
SMILES Code : O=C(OC(C)(C)C)NCCN(C)N

Safety of [ 161490-19-3 ]

Application In Synthesis of [ 161490-19-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 161490-19-3 ]

[ 161490-19-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 97308-23-1 ]
  • [ 60-34-4 ]
  • [ 161490-19-3 ]
YieldReaction ConditionsOperation in experiment
B. Preparation of N-(2-t-Boc aminoethyl)-1-methyl hydrazine A solution of <strong>[97308-23-1]t-Boc aziridine</strong> (2.1 g, 0.0141 mol) in ether (5 mL) was added dropwise to ice-cooled N-methyl hydrazine (6.75 g, 0.141 mol) over a period of 1 h. The reaction mixture was stirred at room temperature for an additional 12 hours. All the volatiles were removed under reduced pressure to yield a thick liquid. This product was used in the next step without any further purification. Yield: 2.5 g (96 percent). 1 H NMR (CDCl3): delta 1.5 (s, 9H, C--Me), 2.4 (s, 3H, N--Me), 2.5 (t, 2H, Me--N--CH2), 2.9 (s, 2H, N--NH2), 3.4 (m, t-Boc--NH--CH2) and 5.4 (bs, 1H, NH-t-Boc). M.S.: [M+H]+ =190.
 

Historical Records

Technical Information

Categories