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Chemical Structure| 1609409-53-1 Chemical Structure| 1609409-53-1

Structure of 1609409-53-1

Chemical Structure| 1609409-53-1

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Product Details of [ 1609409-53-1 ]

CAS No. :1609409-53-1
Formula : C20H22N2O6
M.W : 386.40
SMILES Code : O=C(OCC)C(=O)C1=C(O)C(=O)N(C2=CC=C(C=C2)N3C(=O)CCCC3)CC1
MDL No. :N/A

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Application In Synthesis of [ 1609409-53-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1609409-53-1 ]

[ 1609409-53-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 545445-44-1 ]
  • [ 1609409-53-1 ]
  • 2
  • [ 545445-44-1 ]
  • [ 4755-77-5 ]
  • [ 1609409-53-1 ]
YieldReaction ConditionsOperation in experiment
90% EXAMPLE 1 Preparation of ethyl {5-hydroxy-6-oxo-l-[4-(2-oxopiperidin-l-yl)phenyl] -1,2,3,6- tetrahydropyridin-4-yl}(oxo)acetate. 5,6-Dihydro-3-(4-mophiholinyl)-l-[4-(2-oxo-l-piperidinyl)phenyl]-2(lH)-pyridinone (100 gm) is stirred with Ethyl oxalyl chloride (42.24 gm) in dichloromethane (800 ml) in the presence of Pyridine (26.7 gm) at 25-30C for 3 hrs. After the reaction completion dichloromethane is distilled completely and Ethyl acetate (100 ml) is added. To this 10 % HCI solution (500 ml) is added and stirred for 1 nr. The solid is filtered and dried. Yield 90%
 

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