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Chemical Structure| 15791-90-9 Chemical Structure| 15791-90-9

Structure of 15791-90-9

Chemical Structure| 15791-90-9

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Product Details of [ 15791-90-9 ]

CAS No. :15791-90-9
Formula : C7H8N2O3
M.W : 168.15
SMILES Code : O=C(NN)C1=CC(O)=CC=C1O
MDL No. :MFCD01921944

Safety of [ 15791-90-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H319
Precautionary Statements:P264-P270-P280-P301+P312+P330-P305+P351+P338-P337+P313-P501

Application In Synthesis of [ 15791-90-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 15791-90-9 ]

[ 15791-90-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2150-46-1 ]
  • [ 15791-90-9 ]
YieldReaction ConditionsOperation in experiment
With hydrazine hydrate; In methanol;Reflux; Inert atmosphere; General procedure: Hydrazine hydrate (5 mL, 40%) was added to a solution of requiredester (5.0 mmol) in methanol (20 mL). The solution was refluxed for12-24 h and monitored by TLC until starting material was completelyconsumed. After that, solvent was evaporated under reduced pressureand a small amount of water (5 mL) was added to precipitate the hydrazide,which was filtered and dried in vacuum to give a shiny white toyellow solid in excellent yields, without further purification.
 

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